HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Fluoroaniline → 4'-Fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Fluoroaniline | HCID 9731 | — |
| Edukt | 5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid | HCID 227638 | — |
| Produkt | 4'-Fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide | HCID 19760311 | 60,7% |
Reaktionsschritte
In a manner analogous to Example 1, 2 g of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalene-carboxylic acid and 1 g of 4-fluoroaniline were used to obtain 1.7 g of 4'-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide in colorless crystals. m.p. 163° C.-165° C. (from ethyl acetate/hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05128470 |
| Quelldatensatz | uspto-grants-1992_07 |
| ORD ID | ord-8686e89e6f324c5c9d4bff1bfd4590c3 |
| Quellennotiz | uspto-grants-1992_07 |