Heptane → Toluene heptane

HRID 653847

Reaktionsgleichung

Reaktionsgleichung von HRID 653847
BrC1C=C(Br)C=CC=1OP(OC1C=CC(Br)=CC=1Br)(OC1C=CC(Br)=CC=1Br)=O.[CH3:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].BrC1C=C(Br)C=CC=1O>C1(C)C=CC=CC=1>[CH3:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].[C:31]1([CH3:30])[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1

Komponenten

5

Edukt 3

HCID 8900HeptaneHCID 120052,4-DibromophenolHCID 14670658Phenol, 2,4-dibromo-, phosphate (3:1)

Produkt 1

HCID 22263336Toluene heptane

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

Two hundred and eighty-four grams of crude tris-(2,4-dibromophenyl)phosphate were mixed with 808 grams of a solution of 85% n-heptane and 15% toluene as above. The liquid portion weighed 733 grams and contained 0.047% 2,4-dibromophenol, 1.45% ester product and 0.06% chloridates.

Quellen und Nachweise

ORD-Eintrag
ord-555e4b438369405a8d9ce68fee2899ca
Quelldatensatz
uspto-grants-1992_07
Patentnummer
US05128496

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