HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Ethyl 3,5-dimethyl-4-hydroxybenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 4-Hydroxy-3,5-dimethylbenzoic acid | HCID 138387 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Ethyl 3,5-dimethyl-4-hydroxybenzoate | HCID 3027494 | — |
Reaktionsschritte
A mixture of 500 mg (3 mmol) of 4-hydroxy-3,5-dimethylbenzoic acid, 20 ml of absolute ethanol and a catalytic amount of anhydrous HCl was heated at reflux for 2 h. The mixture was then poured into excess cold water and the resultant precipitate was filtered. The precipitate was washed with water and dried in-vacuo to give the title compound as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05130335 |
| Quelldatensatz | uspto-grants-1992_07 |
| ORD ID | ord-494493c611f549bcb599c2de434f9249 |
| Quellennotiz | uspto-grants-1992_07 |