HCID 18962543, Verbindung → HCID 14567647, Verbindung

Reaktionsgleichung

C(OC1C(OCC)=CC=C2C=1C=CN2)C1C=CC=CC=1.C([O:28][C:29]1[C:37]([O:38][CH3:39])=[C:36]2[C:32]([CH:33]=[CH:34][NH:35]2)=[CH:31][CH:30]=1)C1C=CC=CC=1>>[OH:28][C:29]1[C:37]([O:38][CH3:39])=[C:36]2[C:32]([CH:33]=[CH:34][NH:35]2)=[CH:31][CH:30]=1

Komponenten

Edukt 2

HCID 18962543HCID 18962543, Verbindung

HCID 21850161HCID 21850161, Verbindung

Produkt 1

HCID 14567647HCID 14567647, VerbindungAusbeute 86 %

Versuchsvorschrift

This compound is obtained according to the operating method described in Example 1d, in which the 4-benzyloxy-5-ethoxyindole is replaced by 6-benzyloxy-7-methoxyindole. A white powder is obtained (yield: 86%, m.p.=83°-84° C.).

Aufarbeitung

customThis compound is obtained
customA white powder is obtained (yield: 86%, m.p.=83°-84° C.)

Quellen und Nachweise

ORD-Eintrag: ord-c64a791600a94f599edfbbd9731be30e
Quelldatensatz: uspto-grants-1992_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05131911

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