Oxazoline → Oleic Acid

HRID 654412

Reaktionsgleichung

Reaktionsgleichung von HRID 654412
[C:1]([O:20]C)(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].O1CCN=C1>>[C:1]([OH:20])(=[O:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Komponenten

3

Edukt 2

HCID 68157OxazolineHCID 5364509Methyl Oleate

Produkt 1

HCID 445639Oleic AcidAusbeute 6,8 %

Versuchsvorschrift

A blanker oil composition was prepared by melting 56 grams of oxidized hydrocarbon wax ("Idasoil D906") and 24 grams of sodium petroleum sulfonate ("Petrosul H-60 Sod Sulfonate") at approximately 150° F. until a homogeneous solution was obtained. To this mixture was added 200 grams of methyl oleate (Keil chemical), one gram of Di-2-butyl cresol ("Lubrizol 817") and 5 grams of oxazoline-type surfactant ("Alkaterge ® T-IV") and 1 gram of an organic acid salt corrosion inhibitor ("Hostacor E"). The mixture was stirred to provide a homogeneous solution and 680 grams of mineral seal oil ("Grade 45 oil" Sterling Oil and Chemical Company) was added. The resultant mixture was stirred until a uniform solution obtained and at this point 13 grams of oleic acid was added and the stirring continued until a homogeneous solution obtained.

Aufarbeitung

  1. customA blanker oil composition was prepared
  2. customat approximately 150° F.
  3. customwas obtained
  4. customto provide a homogeneous solution and 680 grams of mineral
  5. customseal oil ("Grade 45 oil" Sterling Oil and Chemical Company)
  6. additionwas added

Quellen und Nachweise

ORD-Eintrag
ord-a1c73c02fce64c13a5231ff777ea52ca
Quelldatensatz
uspto-grants-1992_07
Patentnummer
US05132032

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