HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(1-Naphthyl)-4-pentyn-1-ol → 5-(Naphth-1-yl)pentanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(1-Naphthyl)-4-pentyn-1-ol | HCID 19955557 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 5-(Naphth-1-yl)pentanol | HCID 10353200 | — |
Reaktionsschritte
A mixture of 5-(1-naphthyl)-4-pentyn-1-ol (500 ng, 2.37 mmol) and 5% palladium on barium sulfate (5 mg) in ethyl ether (30 ml) was stirred at room temperature under a hydrogen atmosphere for two days. Solvent removal, after filtration through celite, gave the title compound as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05134128 |
| Quelldatensatz | uspto-grants-1992_07 |
| ORD ID | ord-fc1489072aa34dfd8d39a00b9d7dfcbb |
| Quellennotiz | uspto-grants-1992_07 |