Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | 2-Methyl-1-pentene | HCID 12986 | — |
| Edukt | 4-Mercaptophenol | HCID 240147 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-(Hexylthio)phenol | HCID 20086310 | — |
Reaktionsschritte
A 4-(hexylthio)phenol was prepared as follows. In a one liter flask equipped with thermometer, stirring rod and water condenser was added 126 grams of 4-mercaptophenol and 7 grams of toluenesulfonic acid. The flask contents were heated to 60° C. and 93 grams of 2-methyl-1-pentene were added over a fifty minute period. The flask contents were neutralized with 9 grams of Na2CO3 in aqueous solution and decanted. The reaction product was stripped to a pot temperature of 80° C. at 20 millimeters of mercury. It weighed 216 grams.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04128530 |
|---|
| Quelldatensatz | uspto-grants-1978_12 |
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| ORD ID | ord-ab70397f3e6949cf95fb20215605e801 |
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| Quellennotiz | uspto-grants-1978_12 |
|---|
