HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → 4-Chloro-1-naphthol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | 1-Chloro-4-methoxynaphthalene | HCID 606038 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-Chloro-1-naphthol | HCID 11787 | — |
Reaktionsschritte
The known compound 1-chloro-4-methoxynaphthalene is dissolved in 150 ml. of acetic acid and 150 ml. of 48 percent hydrobromic acid, and the mixture is heated at its reflux temperature for 2 hours. The mixture is diluted with 200 ml. of water and cooled to provide 1-chloro-4-hydroxynaphthalene as a crystalline solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04128659 |
| Quelldatensatz | uspto-grants-1978_12 |
| ORD ID | ord-03d39e03caed4569923ddc9bb0d2b986 |
| Quellennotiz | uspto-grants-1978_12 |