HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyladipate → Disodium adipate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyladipate | HCID 12329 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | Disodium adipate | HCID 24073 | — |
Reaktionsschritte
17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04129520 |
| Quelldatensatz | uspto-grants-1978_12 |
| ORD ID | ord-af3c1eef92454c249d5f397014b710cf |
| Quellennotiz | uspto-grants-1978_12 |