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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 66153Erstellt: 25. Oktober 2026

2,6-Dichloroaniline → 3-Benzoyl-2',6'-dichloroacrylanilide

https://huagongshe.com/reaction/66153

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2,6-DichloroanilineHCID 11846—
EduktPentafluoroanilineHCID 13040—
EduktPhosphorus pentachlorideHCID 24819—
Edukt2-Benzoylprop-2-enoic acidHCID 15839051—
Edukt3-(Benzoyl)pentafluoroacrylanilideHCID 85847495—
Produkt3-Benzoyl-2',6'-dichloroacrylanilideHCID 85847494—

Reaktionsschritte

The following additional compounds are prepared by employing PCl5 reagent in accordance with the method of the above Example 6. An analogous quantity of the appropriate benzoylacrylic acid or a substituted benzoylacrylic acid is employed in the manner of the benzoylacrylic acid of Example 5. Likewise, an analogous quantity of the appropriately substituted aniline is employed in the manner of the 2,6-dichloroaniline. Thus, to prepare 3-(benzoyl)pentafluoroacrylanilide, an analogous amount of benzoylacrylic acid is employed and there is used an analogous quantity of pentafluoroaniline in place of the 2,6-dichloroaniline.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04130661
Quelldatensatzuspto-grants-1978_12
ORD IDord-3d7c09b7671b429ca9133e350ed4823e
Quellennotizuspto-grants-1978_12