HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Nitropropane → HCID 178430959, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Nitropropane | HCID 398 | — |
| Edukt | Diethylamine | HCID 8021 | — |
| Edukt | Benzofuroxan | HCID 68075 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 178430959 | HCID 178430959 | — |
Reaktionsschritte
To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04343942 |
| Quelldatensatz | uspto-grants-1982_08 |
| ORD ID | ord-1c8ab1a20a294172a812417cba9eb226 |
| Quellennotiz | uspto-grants-1982_08 |