HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopentadeca-2,14-dien-1-one → Cyclopentadecanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopentadeca-2,14-dien-1-one | HCID 53676690 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Cyclopentadecanone | HCID 10409 | 94% |
Reaktionsschritte
A solution of 1.00 g (4.55 mMole) of cyclopentadeca-2,14-dien-1-one in 20 ml of ethanol was hydrogenated in the presence of 50 mg of palladium on charcoal. Hydrogen uptake (230 ml) was complete after 1 h at 20°. The mixture was filtered, evaporated and distilled to give 0.96 g (94%) of EXALTONE® having b.p. 115°/0.1 Torr; m.p. 65°-66°.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04346023 |
| Quelldatensatz | uspto-grants-1982_08 |
| ORD ID | ord-21dadf26d14a4ba4b795642887de36a9 |
| Quellennotiz | uspto-grants-1982_08 |