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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 67678Erstellt: 24. Oktober 2026

Lauric Acid → 4-lauramidoethyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-one

https://huagongshe.com/de/reaction/67678

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktLauric AcidHCID 3893—
EduktDiethylenetriamineHCID 8111—
EduktPropanoic acid, 2-methyl-3-oxo-, methyl esterHCID 103507—
Produkt4-lauramidoethyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-oneHCID 70548663—

Reaktionsschritte

Into an apparatus similar to that in Example 1, were charged 103.1 g (1 mole) of diethylenetriamine and 116.1 g (1 mole) of methyl 2-formylpropionate. At 130° to 135° C., 18 g of water and 32 g of methanol were distilled off. Then, after addition of 200.3 g (1 mole) of lauric acid, the amide formation was effected at 200° to 210° C. to distil off 18 g of water, leaving behind 4-lauramidoethyl-6-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04346087
Quelldatensatzuspto-grants-1982_08
ORD IDord-215562d10a4b41ed8bc4d4a47d60473d
Quellennotizuspto-grants-1982_08