HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isopropanol → N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isopropanol | HCID 3776 | — |
| Edukt | N-Methyl-D-glucamine | HCID 8567 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | lauric N-chloramide | HCID 19040106 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea | HCID 20527943 | 63% |
Reaktionsschritte
A mixture containing 7 g (30 mmol) of lauric N-chloramide dissolved in 200 ml of isopropanol, was reacted with a solution containing 5.85 g (30 mmol) of N-methyl-D-glucamine in 150 ml of isopropanol, 40 ml of water and 1.2 g (30 mmol) of sodium hydroxide at 50° C. for a period of 1 hour. The reaction mixture was processed in accordance with the procedures described in Example 12 to yield 7.38 g (63% yield) of N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea of the formula ##STR13## having a melting point of 109° C. and the following analysis:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04346233 |
| Quelldatensatz | uspto-grants-1982_08 |
| ORD ID | ord-6e4c9133aa28410ebd9f602f512201ef |
| Quellennotiz | uspto-grants-1982_08 |