Monomethyl terephthalate → Methyl 4-{[(4-hydroxybutyl)amino]carbonyl}benzoate

Reaktionsgleichung

[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][OH:6].[CH3:7][O:8][C:9]([C:11]1[CH:19]=[CH:18][C:14]([C:15](O)=[O:16])=[CH:13][CH:12]=1)=[O:10]>>[OH:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:1][C:15]([C:14]1[CH:18]=[CH:19][C:11]([C:9]([O:8][CH3:7])=[O:10])=[CH:12][CH:13]=1)=[O:16]

Komponenten

Edukt 2

HCID 15513Monomethyl terephthalate

HCID 258684-Amino-1-butanol

Produkt 1

HCID 4381083Methyl 4-{[(4-hydroxybutyl)amino]carbonyl}benzoate

Versuchsvorschrift

The same procedure as a series of reactions of Example 17 was carried out, except that 4-amino-1-butanol was used in place of the compound 16 and 4-(methoxycarbonyl)benzoic acid was used in place of 1H-imidazole-2-carboxylic acid, to obtain the title compound having the following physical properties.

Quellen und Nachweise

ORD-Eintrag: ord-6f66d895942e4a5bb2ba82c0bc8bff89
Quelldatensatz: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08822459B2

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