HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Bromophenethylamine → 4'-(2-Aminoethyl)-3-biphenylcarboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Bromophenethylamine | HCID 533915 | — |
| Edukt | (3-Carbamoylphenyl)boronic acid | HCID 2737814 | — |
| Edukt | Toluene ethanol | HCID 21863594 | — |
| Lösungsmittel | 1,2-Dimethoxyethane | HCID 8071 | — |
| Produkt | 4'-(2-Aminoethyl)-3-biphenylcarboxamide | HCID 58276405 | — |
Reaktionsschritte
The title compound was prepared from 3-(aminocarbonyl)-phenyl boronic acid and 4-bromophenethylamine according to the procedure described for intermediate I-VII-1 with the exceptions that 4:1 PhMe/EtOH was sued as organic solvent (instead of DME) and the chromatographic purification step was omitted. LC/MS (method E) 0.53 min; m/z 241 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08822518B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-d3081091b1fe44fa8a47eb45f5cae40c |
| Quellennotiz | uspto-grants-2014_09 |