(3-Carbamoylphenyl)boronic acid → 4'-(1,3-Dioxolan-2-yl)-3'-(trifluoromethyl)-3-biphenylcarboxamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	(3-Carbamoylphenyl)boronic acid	HCID 2737814	—
Edukt	2-[4-Iodo-2-(trifluoromethyl)phenyl]-1,3-dioxolane	HCID 58276681	—
Lösungsmittel	Toluene ethanol	HCID 21863594	—
Produkt	4'-(1,3-Dioxolan-2-yl)-3'-(trifluoromethyl)-3-biphenylcarboxamide	HCID 67159994	—

Reaktionsschritte

The title compound was prepared from 3-(aminocarbonyl)phenyl boronic acid and 2-[4-iodo-2-(trifluoromethyl)phenyl]-1,3-dioxolane (I-IX-7) according to the procedure described for IX-10, using PhMe/EtOH (4:1) as organic cosolvents. Colorless solid. LC/MS (method A) 2.38 min; m/z 338 (M+H).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08822518B2
Quelldatensatz	uspto-grants-2014_09
ORD ID	ord-46ac662b190145d0b275375fff7109d3
Quellennotiz	uspto-grants-2014_09