Acetic Acid → 3-((2-amino-4-chlorophenyl)thio)-N,N-dimethylpropanamide

Beteiligte Stoffe

Reaktionsschritte

The solution of 2-amino-4-chlorobenzenethiol (824 mg, 5.126 mmol), N,N-dimethylacrylamide (512 mg, 5.162 mmol), and HOAc (1 ml) in CH2Cl2 (10 ml) was stirred at room temperature for 4 days. The solvent was removed and the residue was loaded on silica column and purified to yield a white solid (1.08 g, 83%).

Herkunft & Nachweise