Sodium Hydroxide → HCID 9815420, Verbindung

HRID 704551Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 704551
[OH-].[Na+].[N:3]1([CH2:8][C:9]#[C:10][CH2:11][NH:12][C:13]([NH:15]C(=O)C2C=CC=CC=2)=[O:14])[CH2:7][CH2:6][CH2:5][CH2:4]1>>[N:3]1([CH2:8][C:9]#[C:10][CH2:11][NH:12][C:13]([NH2:15])=[O:14])[CH2:4][CH2:5][CH2:6][CH2:7]1

Komponenten

3

Edukt 2

HCID 14798Sodium HydroxideHCID 15167055HCID 15167055, Verbindung

Produkt 1

HCID 9815420HCID 9815420, Verbindung

Versuchsvorschrift

To a solution of sodium hydroxide (0.1 mol) at 80° C. is added N-[[[4-(1-pyrrolidinyl)-2-butynyl]amino]-carbonyl]-benzamide (4.3 g, 0.015 mol) (Example 1f) in one portion. The solution is allowed to stir for 12 minutes, cooled, extracted with chloroform, dried over magnesium sulfate and concentrated to give an oil which solidifies upon standing; mp 71°-73° C.

Aufarbeitung

  1. temperaturecooled
  2. extractionextracted with chloroform
  3. dry with materialdried over magnesium sulfate
  4. concentrationconcentrated
  5. customto give an oil which

Quellen und Nachweise

ORD-Eintrag
ord-a49f4496bb6d494aacac8bd4e60fca60
Quelldatensatz
uspto-grants-1991_01
Patentnummer
US04988688

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