HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N,N-Diethyl-1,3-propanediamine → N-[3-(diethylamino)propyl]-4,5-bis(4-fluorophenyl)-1H-pyrazole-1-acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N,N-Diethyl-1,3-propanediamine | HCID 61011 | — |
| Edukt | ethyl 4,5-bis(4-fluorophenyl)-1H-pyrazole-1-acetate | HCID 14699554 | — |
| Produkt | N-[3-(diethylamino)propyl]-4,5-bis(4-fluorophenyl)-1H-pyrazole-1-acetamide | HCID 20073281 | 45,4% |
Reaktionsschritte
By a procedure substantially similar to that of Example 14, 8 g (0.023 mol) of ethyl 4,5-bis(4-fluorophenyl)-1H-pyrazole-1-acetate of Example 3 and 34.3 mL (0.22 mol) of diethylaminopropylamine were reacted to produce 4.45 g of N-[3-(diethylamino)propyl]-4,5-bis(4-fluorophenyl)-1H-pyrazole-1-acetamide. The solid product after trituration in water collapsed to a non-crystalline, white, waxy solid upon drying.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04988725 |
| Quelldatensatz | uspto-grants-1991_01 |
| ORD ID | ord-d3b6380771a74693b629e5a61c38f691 |
| Quellennotiz | uspto-grants-1991_01 |