Ammonia → Morpholine-4-carboxamide

HRID 707052

Reaktionsgleichung

Reaktionsgleichung von HRID 707052
[N:1]1([C:7](Cl)=[O:8])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[NH3:10]>CO>[N:1]1([C:7]([NH2:10])=[O:8])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

Komponenten

4

Edukt 2

HCID 222AmmoniaHCID 848104-Morpholinecarbonyl chloride

Produkt 1

HCID 75088Morpholine-4-carboxamide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel2×

Versuchsvorschrift

A solution of morpholine-4-carbonyl chloride (2.0 g) in methanol (10 mL) and 7 N NH3 in methanol (5 mL) was stirred at 45° C. overnight. The mixture was concentrated to give a solid, which was dried under vacuum.

Aufarbeitung

  1. concentrationThe mixture was concentrated
  2. customto give a solid, which
  3. customwas dried under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-2ae19c97422d4561a7a7cd351007e089
Quelldatensatz
uspto-grants-2015_11
Patentnummer
US09174982B2

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