Propyl Acetate → HCID 22155088, Verbindung

HRID 707743

Reaktionsgleichung

Reaktionsgleichung von HRID 707743
[C:1]([O:4][CH2:5][CH2:6][CH3:7])(=[O:3])[CH3:2]>C(O)C>[CH2:1]([OH:3])[CH3:2].[C:1]([O:4][CH2:5][CH2:6][CH3:7])(=[O:3])[CH3:2]

Komponenten

3

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

The dried high DS starch hexanoate described above (Ex. 12, 71.3 g), ethanol (65.2 g), and n-propyl acetate (65.2 g) were charged to a 500 mL round bottom flask, equipped with condenser, overhead stirrer, nitrogen blanket, thermocouple and heating mantle. The mixture was heated to 60° C. for about 1 hr. to form a transparent, low viscosity solution at 30 wt % solids in 50/50 ethanol/n-propyl acetate.

Aufarbeitung

  1. additionwere charged to a 500 mL round bottom flask
  2. customequipped with condenser
  3. temperatureoverhead stirrer, nitrogen blanket, thermocouple and heating mantle

Quellen und Nachweise

ORD-Eintrag
ord-ba198b69b5fb4b6aaa592aab49863e33
Quelldatensatz
uspto-grants-2015_11
Patentnummer
US09175179B2

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