HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → HCID 178443076, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | N-Palmitoylglycine | HCID 151008 | — |
| Edukt | HCID 178419078 | HCID 178419078 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 178443076 | HCID 178443076 | — |
Reaktionsschritte
Using thionyl chloride, N-palmitoyl-Gly was converted to the acid chloride in toluene at room temperature, then reacted with L-histidine using triethylamine as the base. However, only a trace amount of N-palmitoyl-Gly-His formed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09180201B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-3b47184941904363ac92444c72623d0e |
| Quellennotiz | uspto-grants-2015_11 |