HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Chloro-4-ethoxybenzaldehyde → 3-Chloro-4-(pentyloxy)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Chloro-4-ethoxybenzaldehyde | HCID 4770035 | — |
| Edukt | 3-Chloro-4-(pentyloxy)benzaldehyde | HCID 54795207 | — |
| Produkt | 3-Chloro-4-(pentyloxy)benzoic acid | HCID 61379193 | 72% |
Reaktionsschritte
When the product of Step A was substituted for 3-chloro-4-ethoxybenzaldehyde in Example 49, Step A the identical process afforded the title compound in 72% yield. 1H-NMR (CDCl3) 0.92 (tr, 3H); 1.42-1.65 (m, 4H); 1.76-1.9 (m, 2H); 4.08 (tr, 2H, J=6.51 Hz); 6.92 (d, 1H, J=8.7 Hz); 7.95 (dd, 1H, J=2.1, 8.61 Hz); 8.1 (d, 1H, J=2.07 Hz).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09181182B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-d871737a95014a91a973efbae3b28b10 |
| Quellennotiz | uspto-grants-2015_11 |