HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Aminobiphenyl → N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Aminobiphenyl | HCID 7015 | — |
| Edukt | Pyrimidine, 2,4-dichloro-5-methyl- | HCID 74508 | — |
| Produkt | N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine | HCID 22060710 | — |
Reaktionsschritte
In like manner to the preparation of 5-fluoro-N2,N4-bis(3-hydroxyphenyl)-2,4-pyrimidinediamine, 2-aminobiphenyl and 2,4-dichloro-5-methylpyrimidine were reacted to provide N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine. LCMS: ret. time: 30.47 min.; purity: 91%; MS (m/e): 429 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08822685B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-545dcb3821fb4a3cbfe6b60d9b96d913 |
| Quellennotiz | uspto-grants-2014_09 |