HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenylalanine amide → (2S)-3-Phenylpropane-1,2-diamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenylalanine amide | HCID 445694 | — |
| Edukt | 2-Aminopentanenitrile | HCID 10171288 | — |
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Produkt | (2S)-3-Phenylpropane-1,2-diamine | HCID 12699301 | 35% |
Reaktionsschritte
Following the procedure as described in Preparation 11, making variations as required to replace 2-aminopentanenitrile with L-phenylalanineamide to react with lithium aluminum hydride, (S)-3-phenylpropane-1,2-diamine was obtained as a colorless solid in 35% yield: MS (ES+) m/z 151.2 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09187426B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-34b84eebebbb4076b5083de9d6f058a5 |
| Quellennotiz | uspto-grants-2015_11 |