HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → 1,1'-(Benzene-1,3-diyldimethanediyl)bis(1H-pyrrole-2,5-dione)
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | Maleic Anhydride | HCID 7923 | — |
| Edukt | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Edukt | Sodium Acetate | HCID 517045 | — |
| Produkt | 1,1'-(Benzene-1,3-diyldimethanediyl)bis(1H-pyrrole-2,5-dione) | HCID 22712661 | — |
Reaktionsschritte
The general procedure was carried out using maleic anhydride (20.59 g, 210 mmol), m-xylylenediamine (13.62 g, 100 mmol), sodium acetate (1.64 g, 20 mmol), and acetic anhydride (22.46 g, 220 mmol). The resulting compound was purified by column chromatography (97:3 DCM:EtOAc), and the product obtained as a white solid (6.51 g/22%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09193139B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-81cc3d977aad42a1bf6c65241f847a2b |
| Quellennotiz | uspto-grants-2015_11 |