HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Permanganate → 3-Bromo-4-propoxybenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Permanganate | HCID 516875 | — |
| Edukt | 3-Bromo-4-propoxybenzaldehyde | HCID 4770041 | — |
| Produkt | 3-Bromo-4-propoxybenzoic acid | HCID 8707153 | — |
Reaktionsschritte
3-Bromo-4-propoxybenzaldehyde was oxidized by KMnO4, according to the procedure as described in Example 47, Step A, to give the title compound in 96%, as white solid. 1H-NMR (DMSO-d6) 0.98 (t, 3H, J=7.32 Hz); 1.68-1.79 (m, 2H); 4.06 (t, 2H, J=6.39 Hz); 7.14 (d, 1H, J=8.7 Hz); 7.87 (dd, 1H, J=2.07, 8.61 Hz); 8.01 (d, 1H, J=2.04 Hz); 11.2 (broad s, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09193716B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-00aa242b0f914215a0ff0a6ba3995ba8 |
| Quellennotiz | uspto-grants-2015_11 |