Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 6-Bromo-2-naphthalenecarboxylic acid | HCID 4549852 | — |
| Produkt | 6-Bromo-2-naphthoyl chloride | HCID 21879606 | — |
Reaktionsschritte
6-Bromonaphthalene-2-carboxylic acid (25.1 g) was suspended in thionyl chloride (200 mL), stirred at 60° C. for 16 hours and evaporated under vacuum. Solid was dissolved in dichloromethane (50 mL) and evaporated under vacuum, giving 6-bromonaphthalene-2-carbonyl chloride (27.0 g, crude) as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08822430B2 |
|---|
| Quelldatensatz | uspto-grants-2014_09 |
|---|
| ORD ID | ord-73404d95d15c4e4bb1380de649e4b62e |
|---|
| Quellennotiz | uspto-grants-2014_09 |
|---|
