Acetonitrile → HCID 21889441, Verbindung

HRID 720213Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 720213
[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:15])[CH3:14])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([OH:22])(=[O:21])=[O:20])([CH3:3])[CH3:2].C(#N)C.[Ag:26]=O>CC(C)=O>[CH:1]([C:4]1[C:9]([N+:10]([O-:12])=[O:11])=[C:8]([CH:13]([CH3:14])[CH3:15])[CH:7]=[C:6]([CH:16]([CH3:18])[CH3:17])[C:5]=1[S:19]([O-:22])(=[O:21])=[O:20])([CH3:2])[CH3:3].[Ag+:26]

Komponenten

5

Edukt 3

HCID 6342AcetonitrileHCID 92152Silver(II) oxideHCID 218894203-Nitro-2,4,6-tri(propan-2-yl)benzene-1-sulfonic acid

Produkt 1

HCID 21889441HCID 21889441, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 180AcetoneLösungsmittel

Versuchsvorschrift

Into a flask was charged 20 parts by 2,4,6-triisopropyl-3-nitrobenzenesulfonic acid, 80 parts of acetonitrile and 40 parts of acetone, and the mixture was stirred at room temperature for 16 hours. To this was added 7.46 parts of silver oxide and the mixture was stirred for 16 hours at room temperature. The resulting mixture was filtrated and concentrated to obtain 23.68 parts of silver 2,4,6-triisopropyl-3-nitrobenzenesulfonate.

Aufarbeitung

  1. stirringthe mixture was stirred for 16 hours at room temperature
  2. filtrationThe resulting mixture was filtrated
  3. concentrationconcentrated

Quellen und Nachweise

ORD-Eintrag
ord-b6723cc8ef694f04952780b5ed70cd0d
Quelldatensatz
uspto-grants-2006_11
Patentnummer
US07135268B2

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