Dimethylformamide → 2-Methyl-4-(N-ethyl-N-(beta-hydroxyethyl)amino)aniline

Beteiligte Stoffe

Reaktionsschritte

To 50 mg of Rho575 in dimethylformamide, 53 μl of N,N′-diisopropylethylamine was added followed by 78 mg of p-nitrobenzyl chloroformate dissolved in dimethylformamide. The reaction mixture was stirred for 3 days and the solvent was removed in vacuo. The residue was dissolved in chloroform and purified on a Biotage SP4 System with a SNAP 25 g column and a chloroform methanol gradient, to give a pink product.

Herkunft & Nachweise