17-Azido-3,6,9,12,15-pentaoxaheptadecan-1-amine → HCID 66933864, Verbindung

HRID 720866Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 720866
NCCOCCOCC[O:10][CH2:11][CH2:12][NH:13][C:14]([CH2:16][CH2:17][C@H:18]([NH:26][C:27]([C:29]1[CH:34]=[CH:33][C:32]([N:35](C(OCC2C=CC=CC=2)=O)[CH3:36])=[CH:31][CH:30]=1)=[O:28])[C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])=[O:15].NCCO[CH2:51][CH2:52][O:53][CH2:54][CH2:55][O:56][CH2:57][CH2:58][O:59][CH2:60][CH2:61][O:62][CH2:63][CH2:64][N:65]=[N+]=[N-]>>[NH2:65][CH2:64][CH2:63][O:62][CH2:61][CH2:60][O:59][CH2:58][CH2:57][O:56][CH2:55][CH2:54][O:53][CH2:52][CH2:51][O:10][CH2:11][CH2:12][NH:13][C:14]([CH2:16][CH2:17][C@H:18]([NH:26][C:27]([C:29]1[CH:34]=[CH:33][C:32]([NH:35][CH3:36])=[CH:31][CH:30]=1)=[O:28])[C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])=[O:15]

Komponenten

3

Edukt 2

HCID 2189447617-Azido-3,6,9,12,15-pentaoxaheptadecan-1-amineHCID 66910315HCID 66910315, Verbindung

Produkt 1

HCID 66933864HCID 66933864, Verbindung

Versuchsvorschrift

Compound 26 was synthesized by an analogous procedure as employed for compound 12, but using 1-amino-17-azido-3,6,9,12,15-pentaoxaheptadecane instead of 1-amino-11-azido-3,6,9-trioxaundecane in the first step of synthesis.

Aufarbeitung

  1. customin the first step of synthesis

Quellen und Nachweise

ORD-Eintrag
ord-57776329f171465b94437c39b22d8ba7
Quelldatensatz
uspto-grants-2006_11
Patentnummer
US07135550B2

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