HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl vinyl sulfone → 1-(2-Methanesulfonyl-ethyl)-4-(4-nitro-phenyl)-[1,4]diazepane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl vinyl sulfone | HCID 19354 | — |
| Edukt | 1-(4-Nitrophenyl)-1,4-diazepane | HCID 5055950 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 1-(2-Methanesulfonyl-ethyl)-4-(4-nitro-phenyl)-[1,4]diazepane | HCID 68979613 | — |
Reaktionsschritte
A mixture of 1-(4-Nitro-phenyl)-[1,4]diazepane (4.90 g), Methansulfonyl-ethene (2.35 g) and Methanol (50 mL) was stirred for 2 h at room temperature. The volatiles were removed in vacuo. The product with the molecular weight of 327.40 (C14H21N3O4S) was obtained in this way; MS (ESI): 328 (M+H+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08828991B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-f675f3baab6544c48293dbeb4ed82bcd |
| Quellennotiz | uspto-grants-2014_09 |