Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Thioacetamide | HCID 2723949 | — |
| Edukt | 3-Methoxy-4-nitrobenzohydrazide | HCID 21883875 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | HCID 178488187 | HCID 178488187 | — |
Reaktionsschritte
The mixture consisting of 590 mg g of 3-methoxy-4-nitrobenzoic hydrazide, 6 ml of pyridine and 210 mg of thioacetamide was heated to 95° C. for 2 hours. After cooling, the volatile fractions were removed under reduced pressure at 40° C. and the residue was subjected to column chromatography purification (silica gel, solvent: 95:5 dichloromethane:methanol)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07138414B2 |
|---|
| Quelldatensatz | uspto-grants-2006_11 |
|---|
| ORD ID | ord-1b016a8858ed40a18d46df865caf42b4 |
|---|
| Quellennotiz | uspto-grants-2006_11 |
|---|
