HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(3-Methyl-5-(2-nitrophenyl)-4H-1,2,4-triazol-4-yl)benzoic acid → 2-(3-(2-Aminophenyl)-5-methyl-4H-1,2,4-triazol-4-yl)benzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(3-Methyl-5-(2-nitrophenyl)-4H-1,2,4-triazol-4-yl)benzoic acid | HCID 21883887 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-(3-(2-Aminophenyl)-5-methyl-4H-1,2,4-triazol-4-yl)benzoic acid | HCID 21883868 | — |
Reaktionsschritte
was prepared by hydrogenating 400 mg of 2-[3-methyl-5-(2-nitrophenyl)-[1,2,4]triazol-4-yl]benzoic acid in the presence of Pd/C in tetrahydrofuran and purified by stirring with dichloromethane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07138414B2 |
| Quelldatensatz | uspto-grants-2006_11 |
| ORD ID | ord-197ab0f37be24bf0b716e4cde269af23 |
| Quellennotiz | uspto-grants-2006_11 |