2-Amino-4-chlorophenol → HCID 21884360, Verbindung
Reaktionsgleichung
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[OH:9].[F:10][C:11]1[CH:19]=[CH:18][C:17]([N+:20]([O-:22])=[O:21])=[CH:16][C:12]=1[C:13](Cl)=[O:14]>>[OH:9][C:3]1[CH:4]=[CH:5][C:6]([Cl:8])=[CH:7][C:2]=1[NH:1][C:13](=[O:14])[C:12]1[CH:16]=[C:17]([N+:20]([O-:22])=[O:21])[CH:18]=[CH:19][C:11]=1[F:10]Komponenten
3
Versuchsvorschrift
Prepared by the method of Example 15a), from 2-amino-4-chlorophenol (705 mg, 4.9 mmol) and 2-fluoro-5-nitrobenzoyl chloride (1.00 g, 5.0 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.
Quellen und Nachweise
- ORD-Eintrag
- ord-bfab42c1c66d45c79bf946d8b128c210
- Quelldatensatz
- uspto-grants-2006_11
- Patentnummer
- US07138425B2
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