Propylamine → 2-(3-Nitro-6-propylaminophenyl)-5-trifluoromethylbenzoxazole

HRID 722582

Reaktionsgleichung

[N+:1]([C:4]1[CH:5]=[C:6]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:14]=3[N:15]=2)[C:7](F)=[CH:8][CH:9]=1)([O-:3])=[O:2].[CH2:24]([NH2:27])[CH2:25][CH3:26]>>[N+:1]([C:4]1[CH:5]=[C:6]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:14]=3[N:15]=2)[C:7]([NH:27][CH2:24][CH2:25][CH3:26])=[CH:8][CH:9]=1)([O-:3])=[O:2]

Komponenten

Edukt 2

HCID 7852Propylamine

HCID 218845112-(3-Nitro-6-fluorophenyl)-5-trifluoromethylbenzoxazole

Produkt 1

HCID 218844522-(3-Nitro-6-propylaminophenyl)-5-trifluoromethylbenzoxazole

Versuchsvorschrift

Prepared by the method of Example 54a), from 2-(3-nitro-6-fluorophenyl)-5-trifluoromethylbenzoxazole (218 mg, 0.8 mmol) and propylamine (328 μL, 4.0 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.

Quellen und Nachweise

ORD-Eintrag: ord-716874ddafe94509b9351849d8054af9
Quelldatensatz: uspto-grants-2006_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07138425B2

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