HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Propanediamine → 4-Iodobiphenyl
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Propanediamine | HCID 428 | — |
| Edukt | Sodium Iodide | HCID 5238 | — |
| Edukt | 4-Bromobiphenyl | HCID 7101 | — |
| Lösungsmittel | 1-Pentanol | HCID 6276 | — |
| Produkt | 4-Iodobiphenyl | HCID 15322 | — |
Reaktionsschritte
30 g of 4-bromobiphenyl is dissolved in 40 mL of n-pentanol. 2 equivalents of sodium iodide and 10 mole % of 1,3-propanediamine are added to the 4-bromobiphenyl solution. The reaction mixture is refluxed at 130° C. for sixteen (16) hours to produce 4-iodobiphenyl, as shown in reaction scheme (5).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07138555B2 |
| Quelldatensatz | uspto-grants-2006_11 |
| ORD ID | ord-e26975268c1443fcb894981069a57230 |
| Quellennotiz | uspto-grants-2006_11 |