HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(Trifluoromethyl)benzoic acid → 6-(4-trifluoromethylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(Trifluoromethyl)benzoic acid | HCID 9966 | — |
| Edukt | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| Produkt | 6-(4-trifluoromethylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 53872633 | 35,5% |
Reaktionsschritte
Beginning with 9.2 mg (0.040 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole and 19.2 mg (0.101 mMol) 4-trifluoromethylbenzoic acid, 5.7 mg (35%) of the title compound were recovered as a beige solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05708187 |
| Quelldatensatz | uspto-grants-1998_01 |
| ORD ID | ord-e703032d62fa4d5ab431385d3fd0a54a |
| Quellennotiz | uspto-grants-1998_01 |