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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 728545Erstellt: 24. Oktober 2026

Acetylpyrazine → Propanoic acid [1-(2-pyrazinyl)ethylidene]hydrazide

https://huagongshe.com/de/reaction/728545

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAcetylpyrazineHCID 30914—
EduktPropionylhydrazineHCID 79890—
LösungsmittelEthanolHCID 702—
ProduktPropanoic acid [1-(2-pyrazinyl)ethylidene]hydrazideHCID 5455861764,2%

Reaktionsschritte

A mixture of 6.11 gm (0.05 mole) of 2-acetylpyrazine, 4.41 gm (0.05 mole) of propanoic acid hydrazide and 100 ml of absolute ethanol is refluxed 10 hr. The mixture is cooled. The white crystals which deposit are collected and dried to yield 6.17 gm (64%) of the title compound having a melting point of 181.3° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05049561
Quelldatensatzuspto-grants-1991_09
ORD IDord-634a163bfca84dbcb8aac450056b0f69
Quellennotizuspto-grants-1991_09