HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetylpyrazine → Propanoic acid [1-(2-pyrazinyl)ethylidene]hydrazide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetylpyrazine | HCID 30914 | — |
| Edukt | Propionylhydrazine | HCID 79890 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Propanoic acid [1-(2-pyrazinyl)ethylidene]hydrazide | HCID 54558617 | 64,2% |
Reaktionsschritte
A mixture of 6.11 gm (0.05 mole) of 2-acetylpyrazine, 4.41 gm (0.05 mole) of propanoic acid hydrazide and 100 ml of absolute ethanol is refluxed 10 hr. The mixture is cooled. The white crystals which deposit are collected and dried to yield 6.17 gm (64%) of the title compound having a melting point of 181.3° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05049561 |
| Quelldatensatz | uspto-grants-1991_09 |
| ORD ID | ord-634a163bfca84dbcb8aac450056b0f69 |
| Quellennotiz | uspto-grants-1991_09 |