HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,3-Epoxypropyl 4'-methoxyphenyl ether → HCID 14739881, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,3-Epoxypropyl 4'-methoxyphenyl ether | HCID 16646 | — |
| Edukt | N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide | HCID 14664358 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 14739881 | HCID 14739881 | — |
Reaktionsschritte
To a solution of 2.39 g (13.2 mmol) 1,2-epoxy-3-(4-methoxyphenoxy)propane in 25 mL methanol is added 3.05 g (13.2 g) N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide. The reaction mixture is stirred under a nitrogen atmosphere for 24 h. After this time, the precipitate is collected and recrystallized from ethanol to provide the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05051423 |
| Quelldatensatz | uspto-grants-1991_09 |
| ORD ID | ord-38e8628e4cb44652858f6f795a33044a |
| Quellennotiz | uspto-grants-1991_09 |