Dibutylstannane → Bis(2-acetoxyethyl)dibutyltin

Beteiligte Stoffe

Reaktionsschritte

2.349 g (0.01 mole) of dibutyltin dihydride, 1.722 g (0.02 mole) of distilled vinyl acetate, and 2 g of anhydrous cyclohexane were placed in aPyrex® bowl thermostated at 25° C. The solution was exposed to ultraviolet radiation for 3 hours. The cyclohexane was then eliminated under vacuum at ambient temperature. The expected product was obtained pure in quantitative yield

Herkunft & Nachweise