HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(5-Amino-1-benzofuran-2-yl)ethanone → HCID 11703944, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(5-Amino-1-benzofuran-2-yl)ethanone | HCID 3783367 | — |
| Edukt | 4-Chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide | HCID 68662017 | — |
| Produkt | HCID 11703944 | HCID 11703944 | — |
Reaktionsschritte
The title compound was prepared from 4-chloro-2-methyl-5-phenylisothiazol-3(2H)-one 1,1-dioxide and 1-(5-amino-1-benzofuran-2-yl)ethanone in a similar manner as described for e.g. Examples 9 and 13. 1H NMR (400 MHz, CD3CN): δ 7.89 (bs, 1H), 7.38-7.37 (m, 1H), 7.25 (d, 1H), 7.16-7.10 (m, 4H), 7.09-7.03 (m, 3H), 3.22 (s, 3H), 2.50 (s, 3H); Mass Spectrum: M+H+ 397.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07582629B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-d648d65938054e8298ce91262b6cfa66 |
| Quellennotiz | uspto-grants-2009_09 |