HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cinnamoyl Chloride → (2E)-N-(4-dec-1-ynylbenzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-3-phenylacrylamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cinnamoyl Chloride | HCID 5354261 | — |
| Edukt | 6-[(4-dec-1-ynylbenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one | HCID 11212285 | — |
| Produkt | (2E)-N-(4-dec-1-ynylbenzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-3-phenylacrylamide | HCID 57841371 | — |
Reaktionsschritte
The title compound was prepared following the procedure E using 6-[(4-dec-1-ynylbenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one and (2E)-3-phenylacryloyl chloride. HPLC, Rt: 6.3 min (purity: 95.5%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07589232B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-59108dde39a44841aea02508655a146b |
| Quellennotiz | uspto-grants-2009_09 |