HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoyl chloride → 4-Methoxybenzophenone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoyl chloride | HCID 7412 | — |
| Edukt | Anisole | HCID 7519 | — |
| Produkt | 4-Methoxybenzophenone | HCID 69146 | 47% |
Reaktionsschritte
370 mg of benzoylchloride were reacted with 12 ml anisole to give the benzoylated product 4-methoxybenzophenone in 47% yield. The catalyst used is a HS—AlF3 metal fluoride on a Al2O3 support prepared according to the present invention, which is used in an amount of 300 mg. The reaction is carried out in a discontinuous batch process at 60° C. under reflux with stirring.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07592287B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-a14a8e7438594020a2313d82de28bc73 |
| Quellennotiz | uspto-grants-2009_09 |