Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 73476Erstellt: 24. Oktober 2026

Styrene → Benzene, ethenyl-, polymer with 1,3-butadiene

https://huagongshe.com/de/reaction/73476

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktStyreneHCID 7501—
Edukt1,3-ButadieneHCID 7845—
EduktPotassium HydroxideHCID 14797—
EduktPotassium PersulfateHCID 24412—
EduktPotassium OleateHCID 23665571—
KatalysatorIronHCID 23925—
LösungsmittelWaterHCID 962—
ProduktBenzene, ethenyl-, polymer with 1,3-butadieneHCID 62697—

Reaktionsbedingungen

Temperatur60 °C

Reaktionsschritte

Nine hundred and fifty parts by mass of a butadiene monomer, 50 parts by mass of styrene, 135 parts by mass of deionized water (the concentration of iron: less than 0.02 ppm), 3.0 parts by mass of potassium oleate, 0.3 parts by mass of potassium persulfate, 0.2 parts by mass of tertiary dodecyl mercaptan, and 0.18 parts by mass of potassium hydroxide were placed in a pressure-resistant container with a stirrer. The temperature was raised to 60° C., and polymerization was started. The polymerization was performed for 15 hours to obtain a styrene butadiene rubber latex having a volume average particle size of 80 nm measured by a Microtrack particle size analyzer “nanotrac 150” (trade name) made by NIKKISO CO., LTD. and a solid content of 40% by mass.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08829104B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-65294ff38a9b4bfe8dd3e435431fc7b7
Quellennotizuspto-grants-2014_09