HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
{4-[2-(Diethylamino)ethoxy]phenyl}methanamine → HCID 68816196, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | {4-[2-(Diethylamino)ethoxy]phenyl}methanamine | HCID 235944 | — |
| Edukt | (2-Chloro-4-trifluoromethylphenyl)propynoic acid | HCID 68817422 | — |
| Lösungsmittel | Dichloromethane methanol | HCID 21226129 | — |
| Produkt | HCID 68816196 | HCID 68816196 | — |
Reaktionsschritte
Prepared analogously to Example 2.3.f. from [4-(2-diethylaminoethoxy)phenyl]methylamine and (2-chloro-4-trifluoromethylphenyl)propynoic acid. Yield: 60 mg (22% of theory); melting point: 135° C.-138° C.; C23H24ClF3N2O2 (M=452.90); calc.: molecular ion peak (M+H)+: 453/455; found: molecular ion peak (M+H)+: 453/455; Rf value: 0.4 (silica gel, dichloromethane/methanol (9:1)).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07592373B2 |
| Quelldatensatz | uspto-grants-2009_09 |
| ORD ID | ord-00ab607748f4433d9ace12dca0689b73 |
| Quellennotiz | uspto-grants-2009_09 |