3,5-Dimethylpiperidine → 1-[2-(2-Methoxy-4-nitrophenoxy)ethyl]-3,5-dimethylpiperidine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	3,5-Dimethylpiperidine	HCID 118259	—
Edukt	1-(2-Bromoethoxy)2-methoxy-4-nitrobenzene	HCID 12937254	—
Lösungsmittel	Dichloromethane methanol	HCID 21226129	—
Produkt	1-[2-(2-Methoxy-4-nitrophenoxy)ethyl]-3,5-dimethylpiperidine	HCID 68819560	—

Reaktionsschritte

Prepared analogously to Example 1.1.c. from 1-(2-bromoethoxy)-2-methoxy-4-nitrobenzene and 3,5-dimethylpiperidine. Yield: 0.4 g (48.1% of theory); C16H24N2O4 (M=308.38); calc.: molecular ion peak (M+H)+: 309; found: molecular ion peak (M+H)+: 309; Rf value: 0.5 (silica gel, dichloromethane/methanol (9:1)).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US07592373B2
Quelldatensatz	uspto-grants-2009_09
ORD ID	ord-c7e9ff6246084a478ad9260b6a18f537
Quellennotiz	uspto-grants-2009_09