2-(Trifluoromethyl)benzylamine → N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(trifluoromethyl)-benzyl]amine

HRID 735997

Reaktionsgleichung

Reaktionsgleichung von HRID 735997
[CH2:1]([O:13][C:14]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[C:17]([CH:24]=O)=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[F:26][C:27]([F:37])([F:36])[C:28]1[CH:35]=[CH:34][CH:33]=[CH:32][C:29]=1[CH2:30][NH2:31]>>[CH2:1]([O:13][C:14]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[C:17]([CH2:24][NH:31][CH2:30][C:29]2[CH:32]=[CH:33][CH:34]=[CH:35][C:28]=2[C:27]([F:26])([F:36])[F:37])=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Komponenten

3

Edukt 2

HCID 764472-(Trifluoromethyl)benzylamineHCID 858412014-(Dodecyloxy)-1-naphthaldehyde

Produkt 1

HCID 67187285N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(trifluoromethyl)-benzyl]amine

Versuchsvorschrift

The same procedure as employed in the preparation of Example 394 (step b) but using 4-(dodecyloxy)-1-naphthaldehyde and 2-(trifluoromethyl)benzylamine gave the title compound as an oil. HPLC (Condition A), Rt: 5.54 min (HPLC purity: 98.0%).

Aufarbeitung

  1. customThe same procedure as employed in the preparation of Example 394 (step b)

Quellen und Nachweise

ORD-Eintrag
ord-c0e8d93f9b7d4f91b93b759d75bdac89
Quelldatensatz
uspto-grants-2009_09
Patentnummer
US07592477B2

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