3,4-Dichlorophenethylamine → N-[2-(3,4-dichlorophenyl)ethyl]-N-{[4-(dodecyloxy)-1-naphthyl]methyl}amine

HRID 736001

Reaktionsgleichung

Reaktionsgleichung von HRID 736001
[CH2:1]([O:13][C:14]1[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[C:17]([CH:24]=O)=[CH:16][CH:15]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[Cl:26][C:27]1[CH:28]=[C:29]([CH2:34][CH2:35][NH2:36])[CH:30]=[CH:31][C:32]=1[Cl:33]>>[Cl:26][C:27]1[CH:28]=[C:29]([CH2:34][CH2:35][NH:36][CH2:24][C:17]2[C:18]3[C:23](=[CH:22][CH:21]=[CH:20][CH:19]=3)[C:14]([O:13][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[CH:15][CH:16]=2)[CH:30]=[CH:31][C:32]=1[Cl:33]

Komponenten

3

Edukt 2

HCID 2179583,4-DichlorophenethylamineHCID 858412014-(Dodecyloxy)-1-naphthaldehyde

Produkt 1

HCID 67187143N-[2-(3,4-dichlorophenyl)ethyl]-N-{[4-(dodecyloxy)-1-naphthyl]methyl}amine

Versuchsvorschrift

The same procedure as employed in the preparation of Example 394 (step b) but using 4-(dodecyloxy)-1-naphthaldehyde and 2-(3,4-dichlorophenyl)ethylamine gave the title compound as an oil. HPLC (Condition A), Rt: 5.72 min (HPLC purity: 82.0%).

Aufarbeitung

  1. customThe same procedure as employed in the preparation of Example 394 (step b)

Quellen und Nachweise

ORD-Eintrag
ord-808fbff75d13439b84e0bf1fcf29576c
Quelldatensatz
uspto-grants-2009_09
Patentnummer
US07592477B2

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